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[求助]
請問cau-17以甲醇為溶劑時如何溶解? 已有1人參與
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1.甲醇為溶劑時,加入五水硝酸鉍和均苯三酸后,溶液不是透明澄清的,如何使它透明澄清? 2.cau-17如何達到六棱柱的形貌? 謝謝各位大佬! 發(fā)自小木蟲IOS客戶端 |
專家顧問 (文壇精英)
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Synthesis was carried out under solvothermal conditions in a Biotage Initiator microwave oven with 10 mL vials. Suitable single crystals were obtained by mixing H3BTC (62.5 mg, 297 μmol) and ground Bi(NO3)3·5H2O (125.5 mg, 259 μmol) with 5 mL of MeOH at room temperature. The sealed glass vial was shaken by hand for 1 min and subsequently heated in the microwave oven to 120 °C for 20 min with 600 rpm stirring. 原文沒說要得到澄清溶液吧,室溫時不是透明澄清,也許達到反應溫度就澄清了 |

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