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[求助]
有人懂反相微乳液法,求幫助。。
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Two reverse microemulsions with ω (mole ratio between water and surfactant [CO520 and Triton X-100)] = 5.8 were fabricated by individually adding 75 μL of FeCl3 (527.6 × 10−3 m) aqueous solution or 75 μL of DSCP (527.6 × 10−3 m) aqueous solution into 2.5 mL cyclohexane solution containing 0.03 m CO520/0.26 m Triton X-100/1.14 m 1-hexanol under vigorous stirring. Additionally, 10 μL triethylamine (TEA) was added into the mixed microemulsion for further 10 min stirring. After adding ethanol as emulsion breaker, Fe-DSCP NCP nanoparticles were deposited and collected by centrifugation. The obtained Fe-DSCP nanoparticles were washed with ethanol to purification. 以上是文獻的方法,我遇見的問題是,DSCP很難溶解,并且文獻里反應時間什么的不太明確,破乳加的乙醇量也不知道,感覺無從下手,有懂的大神可以提示一二嗎? 萬分感謝! |
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