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[求助]
求助xrd的sio2PDF卡片，00-059-0336，00-052-0784 已有1人參與
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新蟲 (正式寫手)
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- 專業(yè): 樣品前處理方法與技術(shù)
2樓2019-01-16 00:04:47
ddtongda 
新蟲 (著名寫手)
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【答案】應(yīng)助回帖
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PDF#00-052-0784: QM=Star(S); d=Diffractometer; I=Diffractometer Chabazite SiO2 Radiation=CuKa1 Lambda=1.54056 Filter=Ge Calibration=External(Si) 2T=9.635-85.742 I/Ic(RIR)= Ref: Lightfoot, P., Univ. of St. Andrews, Dept. of Chemistry, Fife, Scotland, UK. ICDD Grant-in-Aid (2000) Rhombohedral - (Unknown), R-3 (148) Z=76 mp= CELL: 13.5226 x 13.5226 x 14.7325 <90.0 x 90.0 x 120.0> P.S=hR76 (?) Density(c)=3.250 Density(m)=3.56A Mwt=60.08 Vol=2333.07 F(30)=54.1(.0135,41/0) Ref: Diaz-Cabamas, P., Barrett, M., Camblor, M. Chem. Commun. (Cambridge), v17 p1881 (1998) Strong Lines: 9.17/X 6.76/3 4.24/2 5.44/1 4.91/1 2.87/1 3.51/1 3.38/1 NOTE: Hydrothermal reaction. 2-Theta d(?) I(f) ( h k l) Theta 1/(2d) 2pi/d n^2 9.635 9.1719 100.0 ( 1 0 1) 4.818 0.0545 0.6850 13.082 6.7621 26.3 ( 1 1 0) 6.541 0.0739 0.9292 14.195 6.2341 4.2 ( 0 1 2) 7.098 0.0802 1.0079 16.282 5.4396 12.5 ( 0 2 1) 8.141 0.0919 1.1551 18.051 4.9102 11.5 ( 0 0 3) 9.026 0.1018 1.2796 19.354 4.5826 2.9 ( 2 0 2) 9.677 0.1091 1.3711 20.939 4.2391 24.4 ( 2 1 1) 10.469 0.1179 1.4822 22.363 3.9722 2.4 ( 1 1 3) 11.182 0.1259 1.5818 22.763 3.9033 2.8 ( 3 0 0) 11.382 0.1281 1.6097 23.429 3.7939 2.5 ( 1 2 2) 11.715 0.1318 1.6561 25.335 3.5126 8.5 ( 1 0 4) 12.668 0.1423 1.7888 26.351 3.3794 7.5 ( 2 2 0) 13.176 0.1480 1.8593 28.110 3.1718 0.2 ( 1 3 1) 14.055 0.1576 1.9810 28.611 3.1174 1.8 ( 0 2 4) 14.306 0.1604 2.0155 30.051 2.9713 1.5 ( 3 1 2) 15.025 0.1683 2.1146 31.135 2.8702 11.3 ( 4 0 1) 15.568 0.1742 2.1891 31.589 2.8300 5.2 ( 2 1 4) 15.795 0.1767 2.2202 32.119 2.7845 1.3 ( 2 2 3) 16.060 0.1796 2.2565 32.897 2.7204 1.3 ( 0 4 2) 16.449 0.1838 2.3097 34.005 2.6343 1.2 ( 2 0 5) 17.002 0.1898 2.3851 35.092 2.5551 2.8 ( 4 1 0) 17.546 0.1957 2.4591 35.542 2.5238 0.9 ( 2 3 2) 17.771 0.1981 2.4896 36.627 2.4515 2.4 ( 1 2 5) 18.313 0.2040 2.5630 38.946 2.3107 0.7 ( 0 5 1) 19.473 0.2164 2.7192 38.946 2.3107 0.7 ( 1 1 6) 19.473 0.2164 2.7192 39.291 2.2912 0.9 ( 4 0 4) 19.645 0.2182 2.7423 39.713 2.2678 0.7 ( 4 1 3) 19.857 0.2205 2.7706 39.935 2.2557 0.7 ( 3 3 0) 19.968 0.2217 2.7855 40.383 2.2317 1.7 ( 5 0 2) 20.192 0.2240 2.8154 42.635 2.1189 0.6 ( 4 2 2) 21.317 0.2360 2.9653 43.512 2.0782 1.5 ( 5 1 1) 21.756 0.2406 3.0234 43.512 2.0782 1.5 ( 0 4 5) 21.756 0.2406 3.0234 44.189 2.0479 1.6 ( 3 3 3) 22.095 0.2442 3.0681 44.772 2.0226 0.6 ( 1 5 2) 22.386 0.2472 3.1065 45.853 1.9774 0.6 ( 0 5 4) 22.926 0.2529 3.1775 46.482 1.9521 0.5 ( 6 0 0) 23.241 0.2561 3.2187 47.608 1.9085 0.8 ( 4 3 1) 23.804 0.2620 3.2922 47.867 1.8988 0.6 ( 2 4 4) 23.933 0.2633 3.3090 48.516 1.8749 1.5 ( 5 2 0) 24.258 0.2667 3.3512 49.688 1.8334 1.7 ( 5 0 5) 24.844 0.2727 3.4271 50.114 1.8188 0.9 ( 0 1 8) 25.057 0.2749 3.4546 51.545 1.7716 1.9 ( 1 6 1) 25.773 0.2822 3.5466 51.545 1.7716 1.9 ( 4 1 6) 25.773 0.2822 3.5466 51.620 1.7692 1.9 ( 4 2 5) 25.810 0.2826 3.5514 52.124 1.7533 0.7 ( 5 2 3) 26.062 0.2852 3.5836 52.693 1.7357 0.7 ( 6 1 2) 26.346 0.2881 3.6200 53.901 1.6996 0.7 ( 1 2 8) 26.951 0.2942 3.6969 54.218 1.6904 1.4 ( 4 4 0) 27.109 0.2958 3.7170 55.281 1.6604 1.1 ( 3 3 6) 27.640 0.3011 3.7841 56.163 1.6364 0.9 ( 0 0 9) 28.081 0.3055 3.8396 57.017 1.6139 1.3 ( 6 2 1) 28.508 0.3098 3.8932 57.895 1.5915 0.4 ( 1 1 9) 28.947 0.3142 3.9480 59.195 1.5596 0.5 ( 0 4 8) 29.598 0.3206 4.0287 60.594 1.5269 1.1 ( 6 1 5) 30.297 0.3275 4.1150 60.594 1.5269 1.1 ( 6 0 6) 30.297 0.3275 4.1150 61.363 1.5096 0.4 ( 3 0 9) 30.681 0.3312 4.1622 62.227 1.4907 0.1 ( 5 2 6) 31.113 0.3354 4.2149 62.227 1.4907 0.1 ( 5 4 1) 31.113 0.3354 4.2149 63.868 1.4563 0.8 ( 0 8 1) 31.934 0.3433 4.3145 64.855 1.4365 0.5 ( 8 0 2) 32.427 0.3481 4.3740 65.593 1.4221 0.6 ( 2 6 5) 32.797 0.3516 4.4182 67.340 1.3894 0.9 ( 5 4 4) 33.670 0.3599 4.5222 67.950 1.3784 1.1 ( 4 1 9) 33.975 0.3627 4.5583 68.693 1.3653 0.6 ( 8 1 1) 34.346 0.3662 4.6021 70.401 1.3363 0.9 ( 4 5 5) 35.200 0.3742 4.7019 71.141 1.3242 0.5 ( 3 3 9) 35.571 0.3776 4.7449 71.628 1.3164 0.8 (4,0,10) 35.814 0.3798 4.7730 72.584 1.3014 1.1 ( 9 0 0) 36.292 0.3842 4.8280 73.708 1.2843 0.7 ( 8 1 4) 36.854 0.3893 4.8923 75.543 1.2576 0.6 ( 9 0 3) 37.771 0.3976 4.9962 76.640 1.2423 0.7 ( 1 8 5) 38.320 0.4025 5.0577 78.474 1.2178 0.5 ( 2 6 8) 39.237 0.4106 5.1595 78.474 1.2178 0.5 (0,4,11) 39.237 0.4106 5.1595 79.646 1.2028 0.6 ( 3 7 5) 39.823 0.4157 5.2238 81.081 1.1851 0.5 ( 5 5 6) 40.540 0.4219 5.3018 81.081 1.1851 0.5 ( 3 8 1) 40.540 0.4219 5.3018 81.833 1.1761 0.8 ( 4 4 9) 40.916 0.4251 5.3424 82.826 1.1645 0.5 ( 6 5 4) 41.413 0.4294 5.3956 84.143 1.1496 0.5 ( 9 0 6) 42.071 0.4349 5.4655 85.742 1.1322 0.5 ( 4 6 7) 42.871 0.4416 5.5495 |
3樓2019-01-17 09:34:34
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